qPCR 2007 Symposium POSTER Presentations


Abstracts - Poster presentations

 

Main Session:   microRNA – siRNA Applications

Poster number   P 001    P 009

Location:           Student Cafeteria


P 001

Regulation of cadmium-induced responses in Arabidopsis thaliana: The role of microRNAs.

Smeets K., Cuypers A., Donckers K., Remans T., Vangronsveld J.

Centre for environmental sciences, Hasselt University, Belgium

Email: karen.smeets@uhasselt.be

As a highly toxic metal, knowledge about cadmium-induced pathways in plants is rather scarce. Cadmium does appear to provoke several oxidative stress related effects, similar to other heavy metals. Because of its non-redox active nature, the induced redox disequilibrium has to be established via indirect pathways. A specific role of this increased ROS-content in the regulation in cadmium-induced responses, however, remains to be elucidated.

Therefore, the early effects of cadmium toxicity were examined by performing a complete transcriptome analysis in Arabidopsis thaliana in combination with the analysis of specific cadmium-induced microRNAs. From these results, a highly coordinated expression response can be concluded during moderate cadmium toxicity, in which an increased ROS-content could play a central role. Furthermore, the induced/inhibited regulative genes are already responding after a few hours of exposure and expression is well regulated between the different organs.

In this study environmental realistic exposure concentrations were used, therefore the outcome is highly relevant for further research on heavy metal contamination.


P 002

Efficient and specific quantification of mammalian microRNAs using a novel real-time PCR approach.

Martin Kreutz1, James Qin1, Holger Engel 2, Po-Jen Shih1, Martin Schlumpberger 2, Subrahmanyam Yerramilli1, and Eric Lader1

1QIAGEN Sciences, Germantown, USA and 2QIAGEN GmbH, Hilden, Germany

Email: martin.schlumpberger@qiagen.com

We have developed an efficient and accurate method for transcriptome-wide miRNA quantification using a SYBR Green based, real-time PCR detection system. The miScript System is highly specific and sensitive, and requires very small amounts of input RNA. The system enables detection of miRNAs as well as mRNAs using the same cDNA preparation allowing simultaneous quantification of miRNA and target mRNA.

A single cDNA prep is sufficient for quantification of several miRNAs of interest, avoiding the need to prepare multiple cDNA preps to quantify each miRNA. Use of a single prep eliminates potential variation that could arise during multiple cDNA synthesis reactions. We will demonstrate the application of this technology to miRNA expression profiling in a model human cell-culture system.

This technology offers researchers a sensitive, specific, and easy-to-perform approach for accurate expression profiling of miRNAs using a small amount of total RNA containing miRNAs. A single cDNA prep from a precious RNA sample is sufficient for profiling of all the known miRNAs in a given model system. This is a substantial advance in the state of the art and would be of broad interest to all scientists studying miRNAs and their targets


P 003

Measure of miRNAs in microdissected colorectal tumor tissues: optimization of RNA preparation.

Stefania Gelmini, Marta Tarter, Francesca Salvianti, Claudio Orlando, Lisa Simi, Mario Pazzagli, Pamela Pinzani.

Clinical Biochemistry Unit, Dept. of Clinical Physiopathology, University of Florence, Italy

Email: s.gelmini@dfc.unifi.it

MicroRNAs (miRNAs) are short non-coding RNA molecules involved in gene expression regulation by repressing translation or cleaving RNA transcripts. Recently a connection between miRNAs and cancer was suggested: several authors reported an altered expression of miRNAs in different cancers where they could function as both tumor suppressor or oncogenes. miRNA analysis has generally been performed by microarray techniques in order to identify the specific expression profile involved in different types of cancers. On the basis on known complementary nucleotide sequences, computer-based prediction model have been developed in order to identify the specific target genes of miRNA; several relevant association with target genes, either oncogenes or tumor suppressors, have been found but the genetic pathways under miRNA regulation have still largely to be determined The laser microdissection is the method of choice to collect pure cell population starting from complex tissues. This technique has been already largely used to identify specific expression profile of mRNA in a single cell or in different cell compartment in the same tissue. In order to obtain in a series of microdissected colorectal tumor tissue samples a sufficient quantity of RNA for gene expression analysis and for a specific related miRNA quantification, we have utilized several RNA extraction methods either specific for miRNA (MIRACLE miRNA Isolation kit, Stratagene) or for total RNA by a specific reagent (Trizol, Invitrogen) or by a lysis buffer (Side Step Lysis and Stabilisation Buffer, Stratagene). We have performed a quantitative relative measure of total (18S) and miRNA by Real Time PCR (TaqMan); the miRNA were miR-31 and miR-135-b. These two miRNAs resulted altered in colorectal tumors in comparison to relative normal tissues (Bandres et al, 2006). The relative quantification is obtained normalising to a RNU6b miRNA. All miRNA measurements were performed by TaqMan MicroRNA assay (Applied Biosystem). For the evaluation of total RNA extracted we have used a primers and probe for 18S RNA (Pre-Developed TaqMan Assay Reagents, Applied Biosystem). Results obtained by MIRACLE show high specificity in the miRNAs extraction and high accuracy for their detection starting from about 10 cells/tube. The other techniques (Trizol,Lysis Buffer Stratagene) were able to detect both total RNA and miRNAs with sufficient sensitivity, reproducibility and accuracy, even if the performances of Stratagene buffer was affected, in same cases, by sample interferences due to the presence of DNA or proteins in the lysate. In all samples (n= 5), miR-31 and miR-135-b resulted overexpressed in tumor microdissected samples in comparison in normal paired tissue.


P 004

MicroRNA Expression Signatures as potential Biomarkers in Thyroid Cancer.

Astrid Potratz1, Cara Martin2,3, Simone Guenther1,O’Leary J.23, Orla Sheils2

(1)Applied Biosystems, Applera Deutschland GmbH, Frankfurter Strasse 129b, Darmstadt, Germany; (2)Histopathology, Trinity College, Dublin, Dublin, Ireland; (3)Pathology, Coombe Women's Hospital, Dublin 8, Ireland

Email: GuenthSM@eur.appliedbiosystems.com

Cancer is caused by abnormal cellular proliferation and the inappropriate survival of damaged cells, which may result in tumor formation. Cells have developed several safeguards to ensure a correct and coordinated cell division, differentiation and death. A defect in the regulatory factors, e.g. tumour-suppressor genes and oncogenes, will increase the propability of tumour development.

MicroRNAs (miRNA), short non-coding, single-stranded RNAs, constitute a novel class of negative gene regulators. Specific miRNAs may even control several target mRNAs resulting in diverse and complex biological processes. Recent evidence indicates that miRNAs might also function as physiological tumour suppressors and oncogenes. Repressing the expression of important cancer-related genes, miRNAs might therefore prove a valuable tool in the diagnosis and treatment of cancer.

Thyroid cancer cell line: The expression profiles of 157 miRNAs in thyroid cancer cell lines have been analyzed using the Applied Biosystems TaqMan MicroRNA Assays. Specific miRNA patterns associated with different pathological pathways have been identified, indicating that miRNAs can be used to reliably discriminate between two common triggers of thyroid cancer. The predicted mRNA targets of these differentially expressed miRNAs belonged to genes involved in regulatory molecular functions such as signalling pathways, cell division control and transcription. This correlates nicely with the respective gene expression profiles using the Applied Biosystems Whole Genome Array System. There, genes involved in the MAPK signalling pathway, oncogenesis and transcriptional regulation where shown to be upregulated whereas several cell cycle regulators were found to be down-regulated.

Cervical cancer cell line: The expression profile of 180 miRNAs in two cervical cancer cell lines was studied using TaqMan miRNA Assays. miRNA was extracted using Ambions mirVana miRNA isolation system. miRNA extracted from histologically normal cervical tissue was used as a reference.

A specific different miRNA expression signature in the cancer cell lines was observed compared to normal cervical tissue. Several of these differentially expressed miRNAs are predicted to interact with cell cycle regulatory molecules. These findings highlight the potential importance of miRNA molecules also in cervical cancer.

The determination of miRNA profiles as a new class of biomarkers has the potential to significantly improve diagnostic accuracy and prognostic information.


P 005

Effects of segmental trisomy on the expression of microRNA genes by qRT PCR.

Blatny R., Ivanek R. & Forejt J.

Institute of Molecular Genetics AS CR, Prague, Czech Republic

Email: blatny@biomed.cas.cz

In our pilot study, we have used adult mice of the Ts43H mouse model of human aneuploidy syndromes carrying largest known segmental trisomy of an autosome with more than 300 genes [1]. We were interested in consequences of the segmental gene dosage imbalance on transcription of genes located in the trisomic region (up to 21 genes, depending on the tissue type) in comparison with genes located in the disomic region (up to 15 genes) of the same chromosome.

MicroRNA genes are known to be example of non-codingRNA genes with strong regulatory potential and are therefore candidate genes in study of development of different pathological states including aneuploidy syndromes. We have measured expression levels of three mature microRNA molecules located in a cluster inside of the trisomic region and one mature microRNA located on another chromosome. We have selected brain as our target tissue, since cognitive abilities were shown to be affected in the model [1], and we used liver as a control tissue.

We are reporting significant differences in individual protein-coding genes between control animals and trisomic animals, mainly for genes in the trisomic region. The average expression level of protein-coding genes in the trisomic region was ~1.6-fold in both liver and brain, which corresponds with the altered gene dosage and does not indicate any kind of dosage compensation. In the disomic region, the average expression level was ~1.0-fold in liver and ~0.9-fold in brain, which indicates slight downregulation of the disomic part in brain. However, statistical significance of this difference remains unclear. These findings are generally in agreement with studies on different mammalian models of aneuploidy and contrast with non-additive gene expression reported in some plants and Drosophila melanogaster .

Finally, we are presenting for the first time measurements of gene-dosage effects on microRNA genes in a mammalian genome. The three microRNA genes located in the trisomic region were upregulated ~1.5-fold. However, the microRNA gene located on another chromosome was found downregulated (0.8-fold).

1. Vacik, T., et al., Segmental trisomy of chromosome 17: A mouse model of human aneuploidy syndromes. PNAS, 2005. 102(12): p. 4500-4505.


P 006

MicroRNA profiling of breast cancer using Locked Nucleic Acid (LNA) based technologies.

Jacobsen N.1, Nørholm M.1, Glue C.1, Stahlberg N.1, Eriksen J.2, Svane I. M.2, Flyger H.2, Balslev E.2, Møller S.1, and Litman T.1.

1Exiqon, Vedbaek, Denmark and 2Herlev University Hospital, Herlev, Denmark

Email: jacobsen@exiqon.com

Abnormal expression of microRNAs (miRNAs) in cancer implies that these small ~22-nucleotide molecules play a role in oncogenesis Therefore miRNAs may comprise a novel class of diagnostic and prognostic signatures. Here, we study the global expression profiles of miRNAs in breast cancer and normal adjacent tissue in order to identify possible new biomarkers for breast cancer.

Here, we present miRNA expression profiles from tumor and normal breast tissue, and found numerous differentially expressed miRNAs, including those previously reported to be associated with breast cancer, such as let-7a/d/f, miR-125a/b, miR-21, miR-32, and miR-136. The differential expression profiles from miRCURYTM LNA Arrays have been confirmed using real-time PCR assays. The real-time RT-PCR detection is a useful tool in addition to Northern blot analysis.

We envision that the different platforms compared in the current study will facilitate an efficient workflow for identification of e.g. disease related miRNAs and subsequent development of reliable diagnostic and prognostic assays.


P 007

Comparison of miRNA expression patterns using the total RNA extracted from formalin-fixed paraffin-embedded (FFPE) cells and that extracted from snap frozen.

Li J.1, Smyth P. 1, Flavin R.1, Cahill S. 1, Denning K. 1, Aherne S. 1 Guenther S. 2, O’Leary J. 1, Sheils O1

(1)Department of Histopathology, Institute of Molecular Medicine, St James’s Hospital, Dublin, Ireland. (2)Applied Biosystems, Darmstadt, Germany

Email: GuenthSM@eur.appliedbiosystems.com

Introduction:

Archival formalin-fixed paraffin-embedded (FFPE) tissues represent an abundant source of clinical specimens; however they have limited utility in applications involving analysis of gene expression due to mRNA degradation and modification during fixation and processing. Interestingly, miRNAs are a small class of RNA recently described as playing important roles in gene regulation, yet their robustness in FFPE is largely unknown. This study analyzed 160 miRNAs in paired snap frozen and FFPE cells to investigate if miRNAs may be successfully deteced in archival specimens.

Methods:

N-thy-ori cells were grown to confluence and aliquots with equal cell numbers were (a) snap frozen and (b) formalin fixed and paraffin embedded into a cell block. Total RNA was extracted using protocols: (a)Ambion mirVana miRNA Isolation kit for snap frozen cells, (b)Ambion RecoverAll Total Nucleic Acid Isolation Kit for FFPE cells. The quality and quantity of RNA yields was measured with Nanodrop and TaqMan® microRNA assays, Human Panel-Early Access Kit.

Results:

To achieve 50 ng of total RNA for each RT reaction, 10,000 ng of total RNA (for 200 assays), was extracted from approximately 2x106 FFPE cells and 1.7x105 snap frozen cells. TaqMan® analysis showed a good correlation of miRNA expression pattern between FFPE and snap frozen cells, with R2>0.95. The mean of ΔCts (Cts_FFPE normalized to Cts_snapfrozen) was -1.04107 and the median was -1.152 with p<0.0001. 65.58% of ΔΔCts (ΔCts normalized to ΔCts_mean), 101 out of 154 determined assays, were between +1 and -1. There was some outlying data in performing the comparison between snap frozen and FFPE cells, most notably miR-146 exhibited ~20 fold decreased expression and miR-302b* ~8 fold increased expression.

Conclusion:

miRNA extracted from FFPE blocks was successfully amplified using Q-RT-PCR. The levels of expression of miRNA detected in total RNA extracted from FFPE were higher than that extracted from snap frozen cells when the amounts of total RNA were identical. It seems reasonable to conclude that this phenomenon was most likely caused by methylol cross-links between RNA and protein resulting small RNA molecules being less compromised than their larger counterparts. The majority of miRNAs demonstrated reliable expression levels in FFPE compared with snap frozen paired samples suggesting these molecules might prove to be robust targets amenable to detection in archival material in the molecular pathology setting.


P 008

A new microfluidic Assay for the Analysis of small RNAs.

Marcus Gassmann1 , Hans-Joachim Mollenkopf2, Marc Valer3, Martin Greiner1

1Agilent Technologies, Waldbronn, Germany, 2Max-Planck Institute for Infection Biology, Berlin, Germany and 3Agilent Technologies Inc., Santa Clara, CA, USA

Email: marcus_gassmann@agilent.com

MicroRNAs (miRNAs) are short 20-22-nucleotide RNA molecules that have been identified recently as sequence-specific regulators of many cellular processes such as apoptosis, proliferation and differentiation. Meanwhile hundreds of microRNAs have been discovered in the genomes of animals and plants, but they are only beginning to be classified by their functional roles. One of the major drawbacks is the lack of adequate analytical methods for the analysis of small RNA samples.

Here we describe a Lab-on-a-Chip based assay that is able to perform very sensitive high resolution analyses of small RNA samples on the Agilent 2100 Bioanalyzer instrument. The assay delivers information about integrity, size and concentration of small RNA species. Purified or enriched small RNA fractions, as well as total RNA samples in concentrations can be run in concentrations down to 100 pg/µl.

The Agilent 2100 Bioanalyzer is a microfluidic instrument platform designed for fast separation and quantification of DNA, RNA, and proteins as well as flow cytometric analysis on cells.


P 009

Multiplex microRNA TaqMan® Low Density Array: A High-Throughput Screening Tool for miRNA Profiling.

Yulei Wang, Raymond Samaha

Applied Biosystems, United States of America

Email: wangyy@appliedbiosystems.com

<>MicroRNAs (miRNAs) are an abundant class of endogenous ~ 22-nucleotide (nt) RNAs that have been shown to have critical functions in a wide variety of biological processes, including development, cell proliferation and death, and oncogenesis. Because of their short size and the sequence similarity between family members, developing a genome wide profiling approach that is sensitive and specific is rather challenging. miRNA arrays as well as bead-based approaches have been used for miRNA profiling, however, their detection sensitivity and specificity are typically low. To address these issues we have developed miRNA TaqMan Low Density Arrays (miRNA TLDA), in which highly sensitive and specific miRNA TaqMan® assays targeting 369 individual human miRNAs and 16 endogenous controls are pre-loaded into a 384-well micro fluidic card. The reverse transcription step (RT) can now be performed in a 48-plex fashion and the resulting cDNA loaded into the miRNA TLDA for real-time PCR detection without the need for robotics. We will be presenting applications of this technology in screening biomarkers in clinical samples and cancer cell lines.

 

Main Session:   Single Cell qPCR

Poster number   P 010    P 011

Location:           Student Cafeteria

P 010

Profiling of the TrpC expression pattern in cerebellar Purkinje cells by quantitative single-cell RT-PCR.

Dragicevic E.1,Blum R.2, Hartmann J.1, and Konnerth A.1

1Friedrich-Schiedel Institute of Neuroscience, TU Munich and 2Physiological Institute, Physiological Genomics, LMU Munich

Email: elena.dragicevic@lrz.tu-muenchen.de

The TRPC (Transient Receptor Potential Canonical) cation channel family consists of seven members; TRPC1-7 (Clapham et al. 2001). TRPC subunits are expressed in many brain areas but little is known about their cellular function in neurons. It has been reported that the TRPC1 cation channel is involved in the mGluR1-dependent slow excitatory postsynaptic current (ImGluR) in Purkinje cells (Kim et al., 2003). However, we found that ImGluR can be evoked in TRPC1 knock-out mice. This suggests a role for other TRPC family members in the activation of ImGluR.

To understand the molecular basis of TRPC-mediated postsynaptic currents, we investigated the cell type-specific gene expression patterns and levels of TRPC encoding transcripts in single Purkinje cells of the cerebellum using a quantitative Reverse Transcriptase-PCR (RT-PCR) approach (Durand et al. 2006). In our experiments, single Purkinje cell somata were obtained by whole soma suction from acute cerebellar slices, using microcapillaries. RT-reactions, followed by purification of single cell cDNA material were amplified in a real time PCR device (Lightcycler). Quantification was performed by using high-resolution standard curves, with comparable efficiencies, for each subunit. In parallel, single cell RT-reactions were validated by quantification of the house-keeping gene glyceraldehyde-3-phosphate-dehydrogenase (GAPDH) in a second qPCR reaction using 1/10 amount of the single-cell cDNA. In addition, we use specific TRPC knock-out mutants to correlate the expression levels of TRPC subunits with the corresponding physiological phenotypes in Purkinje cells.

Our findings revealed that the subunit TRPC3 (372 copies/cell) and not TRPC1 (44 copies/cell) is the predominant TRP-family member in Purkinje cells of wild type mice. TRPC4 (10 copies/cell), TRPC6 (4 copies/cell), and TRPC7 (5 copies/cell) have been detected in few copies, while TRPC5 was not detected yet. TRPC1 knock-out mice show the same TRPC subunit expression pattern. The electrophysiological analysis as well as the quantitative single cell RT-PCR experiments are leading to the conclusion that TRPC3 and not TRPC1 is the most likely molecular candidate for ImGluR in cerebellar Purkinje cells of the mouse.

Clapham, D. E., Runnels, L. W., Strubing, C. (2001) The TRP ion channel family. Nat Rev Neurosci 387-96.

Kim, S. J., Kim, Y. S., Yuan, J. P., Petralia, R. S., Worley, P. F., Linden, D. J. (2003) Activation of the TRPC1 cation channel by metabotropic glutamate receptor mGluR1. Nature 426:285-291.

Durand, Marandi, Herberger, Blum & Konnerth (2006) Pflügers Arch. Eur J. of Physiol. 451, 716-726.


P 011

Changes in the gene expression of mRNA transcripts for insulin like growth factor (IGF-I), their receptor (IGF-IR) and facilitative glucose transporter (Glut-I) in IVM oocytes and preimplantation embryos of Buffalo derived from Somatic Cell Nuclear Transfection.

S.C. Gupta, Neelam Gupta, Alok Pandey

National Bureau of Animal Genetic Resources, Karnal, India

Email: guptasc@yahoo.com

For low rate of SCNT derived cloned embryos reaching to normal and viable clones, one hypothesis is that transcription of one or several developmentally important genes is affected by the in vitro environment possibly leading to the disturbance of process of differentiation and organogenesis. Therefore embryos exhibiting abnormal expression of embryonic genes may be an early indication of incomplete reprogramming that could result in lower survival rates. The real-time quantitative polymerase chain reaction (rtqPCR) has overcome the limitations of conventional, time consuming quantitative PCR strategies and has been matured into a routine tool to quantify gene expression levels, following reverse transcription (RT) of mRNA into complementary DNA (cDNA). It is a sensitive and very efficient technique to examine gene transcription patterns in preimplantation embryos. One of the areas of interest in this regard, is the analysis of gene expression patterns in nuclear transfer (NT) embryos to dissect the processes that failed and develop means to overcome the limitations imposed by these factors. The main objective of this study was to develop an easy and rapid method for measuring gene expression in a single cell by real-time PCR without RNA extraction and purification by using cell to cDNA II kit (Ambion). Based on the developed RT-PCR methodology, we constructed cDNA libraries with single matured oocytes at 0h, 6h, 12h, 18h and 24h of maturation and of embryos at different stages of development (2-cell, 4-cell, 8-cell, 16-cell, morula and blastocyst). Real time PCR cycler was performed using Brilliant SYBR Green Q-PCR master mix (Stratagene) to determine more precisely the transcription levels of IGF-I, IGF-II, and Glut-I in SCNT produced buffalo embryos derived from skin fibroblast cells at preimplantation development. The primers of selected genes GAPDH (reference) and IGF-I, IGF-II, and Glut-I (target genes) for expression studies were designed using the Gene Bank sequences within only one exon in the range of 80-200 bp products. Standard curve for reference and all the target genes were developed for the relative quantification of gene expression. IGF-I transcript expression was clearly visible only in matured oocytes. It was elevated up through 12h of the culture and then declined gradually at the end of 24hrs maturation. IGF-IR, was expressed throughout preimplantation development upto the blastocyst stage, while the expression of facilitative glucose transporter (Glut-I) was also expressed in all stages studied. Gene expression analysis of those genes which plays a important role in activation and reprogramming of matured oocytes and cloned embryos would enable us to better understand the early biological events during preimplantation after nuclear transfer.

Session:   Immuno - qPCR

Poster number   P 012    P 013

Location:           Student Cafeteria

P 012

Real-time immuno-PCR: a new perspective for prion blood screening tests.

Ruelle V., ElMoualij B., Heinen E. and Zorzi W.

Center of research on Prion Proteins, University of Liège, 4000, Belgium

Email: v.ruelle@ulg.ac.be

Prion diseases such as Creutzfeldt-Jakob of human, scrapie of sheep and bovine spongiform encephalopathy of cattle are fatal neurodegenerative disorders characterized by behavioural and locomotor changes, cerebral amyloid plaques and spongiform degeneration of the brain1. In 1996, the first case of variant of Creutzfeldt-Jakob disease (vCJD) was diagnosed in the United Kingdom, through the consumption of prion-contaminated meat and borne meal with Bovine Spongiform Encephalopathy (BSE). Since, their number increased whereas cases of BSE were declining. Until the end of January 2007, 158 people were death from vCJD and 7 are still alive2. The potential for transmission of vCJD by blood transfusions was demonstrated experimentally3 prior the apparition of apparent cases of human transmission of vCJD by transfusion4. From December 2004, 3 people are already death following a transfusion of contaminated blood.

The classical techniques used to diagnosed prion protein (Western blot assays and enzyme-linked immunosorbent assays)5 are not sufficiently sensitive to detect the low levels of prion in the blood. Consequently, it is necessary to develop a sensitive technique allowing the diagnosis of prion protein in blood.

In this study, we therefore focussed on the detection of the prion protein in blood by immuno-quantitative-PCR (iqPCR)6. This technique combines the sensitivity of PCR, by an exponential amplification of reporter DNA, and the specificity of the detection of antigens, by antibodies in an ELISA format7-8. To illustrate the advantages of iqPCR, we have compared it with a conventional ELISA technique in experiments aimed at detecting the resistant form of prion protein in human plasma. Using iqPCR, a minute quantity of prion was detected in blood spiked with infected CJD sample with a detection threshold at least 400-fold lower than classical ELISA.

The iqPCR technique being ultra-sensitive, it could be a technique of choice for the development a new blood screening tests allowing the prion protein diagnosis in infected human and animals ; both at ante-mortem and post-mortem stage.


P 013

TSS-mediating staphylococcal toxins: A novel quantitative real-time immuno-PCR approach for ultra-sensitive detection of SEB and TSST-1.

Andreas Fischer1, Thorsten Kuczius2, Christof von Eiff1, Georg Peters1, Karsten Becker1

University Hospital of Münster, Institute of Medical Microbiology, Germany(1) University Hospital of Münster, Institute of Hygiene, Germany(2)

Email: a.fischer@uni-muenster.de

TSS-mediating staphylococcal toxins: A novel quantitative real-time immuno-PCR approach for ultra-sensitive detection of SEB and TSST-1

Staphylococcus aureus is a major human pathogen characterized by a strain-dependent spectrum of virulence factors. One of these is the family of the bacterial pyrogenic toxin superantigens (PTSAg), comprising the toxic shock syndrome (TSS) mediating toxins TSST 1 and staphylococcal enterotoxin B (SEB). As morbidity and mortality from TSS are substantial, early and reliable recognition of TSS is critical. In addition to their nature as superantigens, enterotoxins also function as potent gastrointestinal toxins with a major public health impact.

Immunological methods used until now are known to be limited in sensitivity and specificity, revealing an obvious need for new highly sensitive and specific methods for the detection of staphylococcal toxins. For this reason, two quantitative real time immuno-PCR (qRT-iPCR) approaches for the detection of SEB and TSST-1 have been developed.

The detection of TSST-1 and SEB, respectively, was achieved by coating toxin-specific polyclonal sheep antibodies (ABs) to microtiter plates in order to capture the target superantigens followed by specific detection of the antigen-AB complex. The resulting immunocomplex was subsequently detected using a covalent antibody-DNA complex, which was synthesized using amino-modified and maleimide-activated reporter DNA and N-succinimidyl-S-actyl-thioacetate-modified secondary detection antibodies. Quantitative real-time amplification of the reporter-DNA was performed for final detection of the toxins.

By usage of this qRT-iPCR technique, superantigen toxin was highly reproducible detected at approximately 10 to 100 pg/ml (0,4 to 4 amol/µl), thereby lowering the limit of detection (LOD) of these toxins by a factor of up to 100 compared to commercially available EIAs. Furthermore, qRT-iPCR offers a high versatility, giving the opportunity of adapting the protocol to detect a broad range of antigens, provided that antibodies for the desired antigens are available. Covalent attachment of different reporter-DNAs to specific antibodies could be used to extend the qRT-iPCR to a multiplex detection platform.

Session:   Pre-analytical-Steps

Poster number   P 014    P 022

Location:           Student Cafeteria

P 014

Evaluation of different RNA extraction methods for small quantities tissue from the marine flatworm Macrostomum lignano.

Plusquin M., Smeets K., Geerdens E., Remans T., Cuypers A., Artois T.

Hasselt University, Belgium

Email: michelle.plusquin@uhasselt.be

Highly sensitive techniques for transciptome analysis, such as real-time PCR, microarrays and others currently used in functional genomics require a high integrity and quality of the RNA, as well as reproducibility between replicates of the same tissue. Our test-organism Macrostomum lignano is a small marine flatworm that has an average weight of 350 µg. Because culture of Macrostomum lignano is labour intensive our goal was to isolate RNA from small quantities of sample material. Samples were lysed with different mechanical lyses such as pulverisation, mixing with steal beads and sonication. Total RNA was then extracted using TRI- Reagent ®, as well as commercial kits based on RNA binding to silicon membranes (Qiagen, Roche) or magnetic beads (Invitrogen). RNA concentrations and purity was assessed using a nanodrop ® -ND 1000 UV-Vis Spectrophotometer using a 1 µl aliquot of the total RNA solutions. RNA integrity of the extracted RNA molecules was evaluated in 1 µl using an Agilent 2100 Bioanalyzer with the RNA 6000 Pico labChip® kit.


P 015

Automated RNA extraction using new Agencourt SPRI technology.

Souquet M.

Beckman Coulter, Germany

Email: msouquet@beckman.com

Agencourt RNAdvance is an Agencourt SPRI® paramagnetic bead-based purification system for the isolation and purification of total RNA from cultured eukaryotic cells, tissue or blood. Agencourt RNAdvance is a consistent and automation-friendly method for utilization in downstream microarray and real-time gene expression analysis. This technique reliably delivers high recovery and purity without the need for filtration or centrifugation and is especially well suited for automation using Beckman Coulter Biomek® solutions.


P 016

Advanced Data Mining Software for Applied Biosystems RT-PCR Data Analysis.

de Alarcon P.1 Ferlinz A.2

1Integromics SL, Spain and 2Applied Biosystems

Email: pedro.dealarcon@integromics.com

Great advances in instrumentation, accurate fluorescence detection, improvements in reagents (eg. by means of ABI Taqman probes) and protocols have increased the use as well as the range of applications of quantitative RT-PCR experiments. Nowadays, RT-PCR is the best technique for relative gene expression quantification and it is expanding to other areas like miRNA profiling, biomarker discovery, diagnostics and Copy Number Analysis. Moreover, the amount of data generated is also growing as experiments are being performed within a high-throughput context. In this sense, advanced bioinformatic tools that help researchers in the analysis and interpration of raw data are demanded by the scientific community as a key complement to the instrumentation and reagents. In the present poster, Integromics introduces a new high-performance software specifically designed for the new era of quantitative RT-PCR. The software has been built around four principles, namely: high-throughput statistics and data mining, interactive visualization, functional interpretation and extensible modular approach. State-of-the-art statistics are key to provide quality control and analysis of raw data for filtering of outliers and noisy experiments. Further procedures are provided towards the assesment of expression stability of endogenous genes (like Normfinder), differential expression by means of statistical tests, and clustering techniques for grouping similar expression profiles. All the statistics are implemented in the R language which ensures the capability of dealing with large amounts of data as well as benefiting from the existing libraries in Bioconductor (www.bioconductor.org). The software is implemented as a plugin of Spotfire Decisionsite, a leading application for professional and interactive visualization of multidimensional data. Visualizations in Spotfire facilitate the task of exploring large datasets (possibly with hundreds of genes and samples) so that it becomes easier to pose interactive queries and focus on relevant results. Even more, once the results from the analysis highlight the existence of characteristic expression profiles, it is crucial to enrich the numerical information with functional annotations provided by content repositories like the Panther database (www.pantherdb.org). As mentioned above, RT-PCR is a powerful technique that can be applied in many different contexts like relative quantification, miRNA profiling or genotyping. However, it is unrealistic to provide software that cannot be adapted to such diversity. In this sense, the software implements analytical workflows that can be easily adapted to specific user needs or experimental settings. A workflow is a set of sequential steps that guides the user from the importing of raw data to the final analysis in a very natural manner. This facilitates the use of the tool by non-experts in biostatistics but does not limit its power as statiticians can add or manipulate the procedures contained in the software.


P 017

Preamplification of Sample Limited Specimens for Real-Time Gene Expression Analysis.

Junko Stevens 1, Renata Coudry2, Cynthia Spittle3

1Applied Biosystems, California, US, 2Hospital A C Camargo,Sao Paulo, Brazil and 3Fox Chase Cancer Center, Philadelphia, US

Email: stevenjn@appliedbiosystems.com

Accurate gene expression profiling can be compromised by the quantity of RNA that is isolated from cells or tissues. We have developed a robust solution for uniform amplification of cDNA prior to quantitative, real-time PCR. TaqMan® Preamp Master Mix allows preamplification of up to 100 gene targets simultaneously using the TaqMan® Gene Expression Assays as the source of pooled gene-specific primers. TaqMan assay-based preamplification preserves equilibrium of targets and retains the relative copy numbers of starting targets in a reproducible and precise manner. Preamplification of random-primed cDNA is independent of amplicon distance from the 3’ end, making it amenable to use with partially degraded or viral RNA. Uniformity of preamplification was demonstrated using Laser Capture Micro dissection (LCM) in formalin-fixed, paraffin embedded (FFPE) tissue. RNA extracted from clinical samples was reverse transcribed to cDNA using High Capacity cDNA Reverse Transcription Kit The simple workflow enables researchers to enrich the amount of limited RNA samples uniformly within 1.5 hours.


P 018

qPCR with mRNA isolated from urothelial cells from urine.

Bontrup H., Delbanco J., Bruening T., Johnen G.

BGFA, Bochum, Germany

Email: bontrup@bgfa.ruhr-uni-bochum.de

Objectives

Bladder cancer in chemical workers is an occupational disease associated with previous exposure to aromatic amines. Currently, urine-based markers used for screening of high-risk collectives are not of high sensitivity. To detect cancer at earlier stages more suitable non-invasive markers are necessary. Some promising new tumor markers are based on mRNA quantitation. The aim of this study was to establish and optimize a practical and efficient mRNA isolation method that allows applying qPCR-based assays with urothelial cells from urine.

Methods Six different isolation methods on the basis of commercially available kits were compared using urine samples of healthy donors and a control RNA with known concentration. A situation was simulated comparable to sample collection in a clinical setting. Cells were collected from urine by centrifugation and transferred to a buffer according to the manufactures recommendations. After short (48 h) storage at -20°C the mRNA isolation was performed. In all tested assays mechanical disruption of the cells was identical. The six isolation methods differed by DNA removal step (DNase treatment or special DNA column) and material of the RNA columns. After isolation, extracted RNA was transcribed to cDNA and quantified on a LightCycler system using an adapted Taqman-based assay for ß-Actin (FDI, Malvern, PA, USA). Possible DNA contamination was monitored with “RT-Minus-PCR” control runs.

Results It was possible to establish a system for mRNA isolation from urine but the analysis showed that urine as a starting material yields high contaminations with genomic DNA. Therefore, DNA removal is essential to obtain mRNA of sufficient quality for qPCR. Our results show that DNA could not be removed adequately by DNase digestion. Better yield and purity was only possible with application of a special glass fibre column that selectively binds DNA. This also allows to recover the DNA and use it for other applications.

Conclusions Most of the six tested methods for mRNA isolation from urine are generally suitable for downstream qPCR applications. However, best results can be obtained with a DNA column-based method (INVITEK, Berlin) that avoids DNase treatment. It excelled in two points: Reproducibility of yield even with very small amounts of starting material and reliability in the separation of DNA and mRNA. Both properties are an absolute requirement for field studies where cell material is limited and frequently of varying quality.

This study was in part supported by Fujirebio Diagnostics Inc.


P 019

Quantitative mRNA expression of the embryonic stem cell marker POU2 in early developmental stages of Atlantic cod (Gadus morhua).

Kaja Helvik Skjærven, Elisabeth Holen

National Institute of Nutrition and Seafood Research (NIFES), Norway

Email: ksk@nifes.no

Embryonic stem cells (ESC) from Atlantic cod (Gadhus morhua) have been isolated and cultured successfully. The cultured cells showed characteristic features for ESCs, including spontaneous differentiation and the ability to form embryoid bodies following retinoic acid treatment. In addition the ESCs could be directed to differentiate into neuronal like cells upon stimulation.

Detection of genes that identify ESCs from other differentiated cells is vital for the method. POU2 is one such gene, known to regulate potency, and self renewal in ESCs. Class V POU5f1 genes are found in blastula cells of different species; Oct4 in mammals and POU2 in zebrafish. We have previously described a fragment of POU2 isolated from Atlantic cod that is 100% identical to zebrafish POU2 at the amino acid level, but not at the nucleotide level. Using real-time PCR technique, we report that blastula cells taken from 1 and 1.5 days post fertilization (DPF) express the highest transcriptional levels of POU2. At the early gastrula stage (2 DPF) a 1.5 fold reduction in POU2 expression was correlated to the presence of some early differentiating cells. By the late gastrula stage (3 DPF), POU2 expression was barely detectable, and coincided with the presence of many differentiated cells. We conclude that POU2 can be used as an ESC marker for Atlantic cod, and the method represents an important new research tool for use in marine teleost species.


P 020

Relative mRNA quantification models and the impact of RNA integrity.

Simone Fleige and Michael W.Pfaffl

Physiology Weihenstephan, Center of Life and Food Sciences (ZIEL) Technical University of Munich, 85350 Freising, Germany

Email: fleige@wzw.tum.de

Quantitative real-time PCR has become one of the most widely used methods of gene quantitation. The method exhibits a large dynamic range, boasts tremendous sensitivity, has little to no post-amplification processing, and is amenable to increasing sample throughput. An essential requirement for a successful quantitative mRNA analytics using qRT-PCR is the usage of intact RNA. Low-quality RNA may compromise the derived expression results. The importance of RNA quality for the qRT-PCR was analyzed by determining the RNA quality of different bovine tissues and cell lines (n=11). Diverse artificial and standardized RNA degradation levels were assessed using the capillary electrophoresis system (Agilent Bioanalyzer 2100). The RNA quality was classified according the RNA integrity number (RIN). Further on, a research into the effect of different length of amplified products and RNA integrity on expression analyses was investigated. Degraded RNA interferes with qRT-PCR performance as such, expressed as Ct value, whereas PCR efficiency is minor effected by RNA integrity. Statements about importance of normalization could be confirmed by our investigations, consequently we commended an efficiency-corrected relative quantification strategy and normalization with at least one internal reference gene. We can recommend a RIN higher than five and a PCR product length up to 200 bp as a minimal requirement for a successful and reliable quantitative real-time RT-PCR quantification.


P 021

REPEATABILITY OF HOUSE DUST SAMPLES IN RELATION TO QUANTITATIVE PCR OF MICROBES.

Pasi Kaarakainen1, Asko Vepsäläinen1, Aino Nevalainen1, Teija Meklin1,2

1National Public Health Institute, Department of Environmental Health, Kuopio, Finland and 2Technology Centre Teknia Ltd, Kuopio, Finland

Email: pasi.kaarakainen@ktl.fi

Possible specific associations between fungal species in our indoor environment and adverse health effects, such as respiratory symptoms, asthma and allergy are a major topic of interest. House dust sampling has been used to assess microbial exposures and to describe microbial populations in indoor environments. However, the repeatability or representativeness of such sampling has not been thoroughly validated.

In this study, the repeatability of house dust sampling was tested. Furthermore, the seasonal variation of the microbial populations was analyzed to assess the representativeness of a single sampling. QPCR was used for the identification of 16 species or assay groups of fungi from house dust samples from five houses without any moisture damage. The repeatability of the analysis of a floor dust sample with qPCR was tested by isolating DNA from homogenized dust samples as five parallel samples. Collecting samples in four different seasons enabled the consideration of seasonal variation.

The highest concentrations from analysed species or assay groups of fungi were observed for Aureobasidium pullulans, Penicillium/Aspergillus/Paecilomyces variotii group, Aspergillus penicillioides, Cladosporium herbarum and Cladosporium cladosporioides, respectively. Fungal concentrations varied between seasons depending on analysed species or assay groups. Concentrations of A. pullulans and two Cladosporium species were at their highest in summer and autumn while for Penicillium and Aspergillus species, the differences between different seasons were not so obvious. The repeatability of the parallel isolations of DNA was good for most of the analysed species. The best repeatability was observed for assays of C. herbarum and P. chrysogenum with ICC value (similarity of the parallel samples) 84.5 and 83.1 %, respectively. ICC was over 70 % also for six and over 60 % for three other assays. In summary, our results suggested that qPCR is a promising tool for the microbial analyses from house dust samples in epidemiological studies. In determining the qualitative procedures of the method and the reliability of the results, homogenization of the sample matrix and the number of the repeats of analyses are the primary issues.


P 022

RNA Integrity database: A web repository enabling RNA trace comparisons.

Hans Brunnert1, Martin Greiner1, Marcus Gasmann1, Michael Kim2, Marc Valer2

1Agilent Technologies, Waldbronn, Germany and 2Agilent Technologies Inc, Santa Clara, CA, USA

Email: martin_greiner@agilent.com

Lab-on-a-Chip devices are broadly used for RNA integrity analysis on Micro array and qPCR gene expression analysis. This creates the need and opportunity for users to screen and validate RNA traces for relevance and troubleshooting. Here we describe the design of the backbone as well as examples of use for a new RNA profile web database. The database aims to host a large variety of sample types spanning different genus, tissues and sample treatments, although the database is initially limited to contain bioanalyzer traces. Each electropherogram is annotated with sample source details as well as analytical data like UV, Ribosomal ratios, RIN and more. They also include details on the RNA extraction and the downstream experiment.

By design the database is open to the scientific community: free querying and curated contributions for individuals as well as large batch uploads from core labs. Individuals are able to compare their own results with those of others with similar samples and protocols. It also allows comparison of alternative RNA isolation methods based on its resulting electrophoretic traces.


Session:   qPCR BioStatistics & BioInformatics

Poster number   P 023    P 028

Location:           Student Cafeteria

P 023

GenEx for Real-time PCR Gene Expression Profiling.

Forootan A., Kubista M., Sjögreen B and Andrade J M

TATAA Biocenter, Sweden MultiD Analyses, Sweden Dept of Analytical Chemistry, University of A Coruna Center for Applied Scientific Computing, Lawrence Livermore National Laboratory

Email: amin.forootan@multid.se

The extraordinary sensitivity and virtually unlimited dynamic range of real-time PCR makes it the preferred technology for gene expression profiling. Candidate marker genes are identified by microarray technology and validated on representative samples by real-time PCR. False leads are discarded, resulting in very powerful panels of expression marker. Such panels can be developed for staging of disease, classification of cells, studies of expression pathways, effects of drugs and the like. The recent development of high throughput real-time PCR platforms such as the 384 well plate instruments from Applied Biosystems and Roche, and most recently the 48x48 (2304 wells) microfluidic card from Fluidigm will spur the development further. To extract maximum information from expression profiling experiments powerful statistical and mathematical methods are needed to find correlations between the measured profiles and identify the genes and samples that show common behavior. Here we present GenEx, which is the first windows based package dedicated for real-time PCR expression profiling. GenEx has user-friendly interface that makes advanced analyses really easy. Data from multiplate experiments are readily pre-processed and analyzed by methods such as geNorm , Normfinder, Principal Component Analysis, Hierarchical clustering, Self-Organizing Maps, Potential curves and much more. The results are presented in highly attractive plots.

www.multid.se

The Real-Time Polymerase Chain Reaction, M. Kubista, J.M. Andrade, M. Bengtsson, A. Forootan, J. Jonak, K. Lind, R. Sindelka, R. Sjöback, B. Sjögreen, L. Strömbom, A. Ståhlberg, N. Zoric, Molecular Aspects of Medicine (2006) 27, 95-125


P 024

EM algorithm for gene copy number estimation using TaqMan® assays.

Catalin Barbacioru, Kelly Li, Raymond Samaha and Katherine Lazaruk

Applied Biosystems, Foster City, CA, United States of America

Email: catalin@appliedbiosystems.com

Genetic variation in the human genome takes many forms, ranging from large, microscopically visible chromosome anomalies to single-nucleotide changes. Deletions, insertions, duplications and complex multi-site variants, collectively termed copy number variations (CNVs) or copy number polymorphisms (CNPs), are found in all humans and other mammals. CNVs influence gene expression, phenotypic variation and adaptation by disrupting genes and altering gene dosage, causing diseases, as in microdeletion or microduplication disorders, or confer risk to complex disease traits such as HIV-1 infection and glomerulonephritis.

Recently, TaqMan® gene copy number assays have been developed for detection of genetic variation at gene level using primers and probes designed for genomic DNA sequences. Each well is duplexed with two assays. The FAM dye-based assay is designed to detect the genes-of-interest and the VIC® dye-based assay for detection of the reference gene, RNase P. The difference between FAM and VIC measurements (dCT) is indicative of the relative abundance of the gene-of-interest against 2 copies per diploid genome regardless of the status of the gene-of-interest. In this study, we present an algorithm for gene copy number estimation from TaqMan® gene copy number assays based on EM algorithm for mixtures of normal distributions. After removing technical outliers from data, the algorithm finds maximum likelihood estimates of parameters in probabilistic models, where the model depends on unobserved samples copy number of the gene-of-interest. Estimates of the gene copy number and confidence levels in predicted copy numbers are reported for each sample. Under current protocols, we are capable of distinguishing up to 8 copies of the gene of interest with at least 95% confidence, assuming 100% efficiency of the FAM dye-based assay.

To evaluate this algorithm, we present experimental results for 5 important drug metabolism genes (CYP2D6, CYP2E1, CYP2A6, GSTM1 and GSTT1) on 270 individual samples from International HAPMAP Project representing 4 different populations (Caucasian, African, Chinese and Japanese). Copy number analysis for these genes shows perfect consistency for sample duplicates. Copy number variation (from 0 to 4) is observed for all 5 genes. Significant differences of copy number frequency in these populations are revealed for CYP2A6, CYP2D6, GSTM1 and GSTT1. Therefore, data presented here is most relevant for highlighting variable regions of the genome that warrant consideration in disease studies. Furthermore, combining this data with SNP data for the same genes, we demonstrate that departures from diploidy can cause apparent genotyping failure and give inaccurate genotyping. Therefore, measuring copy number variation in these genes is an important complement to genotyping assays.


P 025

Statistical analysis of relative expression results in real-time PCR: Development of a Relative Expression Software tool (REST-2007©)

Ross Saad1, David Chiew1, Matthew Herrmann1, Valin Reja1, Michael W. Pfaffl2

1Corbett Research, Mortlake, NSW, Australia and 2Technical University Munich, Freising Weihenstephan, Deutschland

Email: michael.pfaffl@wzw.tum.de

REST 2007 is new standalone software for analyzing gene expression using real-time amplification data. The software addresses issues surrounding the measurement of uncertainty in expression ratios by introducing randomization and bootstrapping techniques. New confidence intervals for expression levels also allow measurement of not only the statistical significance of deviations but also their likely magnitude, even in the presence of outliers. Whisker box-plots provide a visual representation of variation for each gene, highlighting potential issues such as distribution skew. REST 2007 builds on its predecessor REST 2005 with significant improvements to randomization algorithms. This new revision introduces alternative data inputs such as single sample efficiency and amplification take-off point, alleviating the need to set amplification plot thresholds.

http://REST.gene-quantification.info/


P 026

Using fuzzy logic algorithm and gene expression database ONCOMINE in COPD outcome forecasting.

Shilov B.V., Bukreeva E.B.

Siberian State Medical University (SSMU), Russian Federation

Email: shilov@ssmu.ru

Chronic obstructive pulmonary disease (COPD) occupies one of the first places in frame of a sickness rate in the world. COPD is a focus of chronic inflammation in organism. Chronic inflammation and its local repeated stress have long been known to be risk factors for cancer. Moreover risk of carcinogenesis increases under influence infectious pathogen. Examples include: Helicobacter pylor bacterial infection and gastric adenocarcinoma; hepatitis B virus and hepato-cellular carcinoma; chronic bowel disease and colon carcinoma; EBV and nasopharyngeal carcinoma in humans. Thus risk of malignant outcome of disease can be enlarged if a patient with COPD has colonization of the infectious agents in his organism.

Infectious agent of inflammation influences on squamous cell methaplasia development in COPD patients. This fact accompanies by increase of squamous cell quantity and rising in brush-biopsies reserved cell number belong in G2 phase of cell cycle. Our investigation included survey of 37 patients with COPD infectious exacerbation. In conditions of similar morphological and pathological changes different patients had various genes expression level.

There is known differences in these genes expression beside healthy humans and malignant disease patients. Dates about these differences were obtained from ONCOMINE database with free access. ONCOMINE, a cancer microarray database and web-based data-mining platform aimed at facilitating discovery from genome-wide expression analyses for elucidation state of indicated genes expression in patients with squamous cell methaplasia. Search and analysis ONCOMINE results we used in fuzzy logic algorithm for expert fuzzy rules forming.

When dealing with gene expression data, the problem is even more complicated, because no expert exists to determine what defines a “normal” expression level. Using fuzzy logic, the full range of expression data is first measured and is then broken into discrete subsections based on the observed data. These discrete subsections then provide a qualitative description of the data.

Use the algorithm has allowed patients classifying on the gene expression basis in groups with different forecast of the upshot of the disease. Three groups were chosen: favorable forecast (5 patients), stabile condition of the chronic inflammation (24 patients) and group with high probability squamous cell methaplasia development (8 patients).


P 027

qRT-PCR applied to the comparative analysis of plant splice variants in time-course water-stress experiments.

Cantale C., Latini A., Sperandei M. and Galeffi P.

BAS BIOTEC GEN, ENEA, Italy

Email: cantale@casaccia.enea.it

The understanding of the plant gene response to the environmental stresses at the transcriptional level is a main challenge for dissecting their role in the stress tolerance. We analysed the expression profile of a DREB-homologous gene, TdDRF1, using Real Time RT-PCR in various different Triticum durum and Triticale cultivars upon dehydration, both in greenhouse and in controlled field experiments. The TdDRF1 gene is alternatively spliced and results in three splice variants, two of them codifying for putative transcriptional activators and the third one producing an abortive putative protein with an unknown function. For each of the examined cultivars, a time-course experiment under water-stress is carried out including two groups, the control plants, that continue to be watered and the stressed plants, that are no more watered. The experiments are carried out using plants at the same growth level and some leaves are collected and pooled at fixed times to average the possible individual and position/soil variability.

The three splice variants, TdDRF1.1, TdDRF1.2 and TdDRF1.3 , are 1455bp, 1367bp and 1314bp respectively and a high sequence identity among the exons in the regions flanking the splicing recognition site prevents the design of primers able to select exclusively each transcript, as demonstrated by the co-amplification observed in experiments using SYBR Green technology. Thus, the qRT-PCR experiments have been carried out using the TaqMan probe-based technology and the 18S rRNA was used as an internal control. It has to be underlined that we were interested in comparing the three transcripts in the same samples of interest. As the expression levels of the three target genes are largely different and one is present in very small amounts, the experimental conditions resulted suboptimal in some cases, as demonstrated by the amplification plots.

Amplification efficiencies of each sample have been evaluated from raw data using LinReg software and show significant differences among the targets. The amplification efficiency of each transcript has been estimated also by linear regression using serial dilution. We report our results obtained using two different methods, Q-gene and a combination of LinReg software and GED formula. The last methodology has been applied using both individual and averaged amplification efficiencies. Furthermore, the application of the GED formula to our data results in three possible data combinations, that are compared and discussed.


P 028

Simplified simulation model of polymerase chain reaction (PCR).

Anneliese Ernst1, Veronique Creach2, Sven Becker3, Lucas J.Stal4, Peter M.J. Herman4.

1Fraunhofer IGB, Stuttgart, Germany, 2Cefas, Lowestoft, UK, 3Max Planck Institut für Limnologie, Plön, Germany and 4NIOO-KNAW, Yerseke, Niederlande

Email: ern@igb.fhg.de

A simplified model of polymerase chain reaction (PCR) is capable to describe essential characteristics of the amplification kinetics of this cyclic reaction. The model is based on the assumption that the PCR is designed and conducted in such a way that (one) PCR primer(s) limit(s) the formation of double-stranded PCR products. The absence of other limiting factors such as nucleotide limitation, enzyme limitation or shortage of the fluorescent dye SYBR Green® greatly reduces the number of parameters required to simulate real-time kinetics of individual amplification reactions in more explicit models. With a self-developed FORTRAN code, we can fit experimental data using the initial concentration of the limiting PCR primer to calibrate the fluorescence emitted by Sybr Green. This fit provides a novel method to estimate the initial concentration of target DNAs in a PCR sample. The method does not rely on external or internal standards. The simulations provide explanations for the occurrence of PCR biases and artifacts; and they are a valuable tool for teaching purposes, and in optimizing PCR protocols.

Session:  New Diagnostic applications with qPCR

Poster number   P 029    P 065

Location:           Student Cafeteria

P 029

Application of qRT-PCR in reproductive toxicology.

Wolfgang R. Schäfer, Wolfgang R. Deppert, Michael Simon, Katrin Roth, Aida Hanjalic-Beck, Claudia Nöthling, Hedwig Austermann-Hesse, Hans Peter Zahradnik

Universitäts-Frauenklinik Freiburg, Germany

Email: wolfgang.schaefer@uniklinik-freiburg.de

Drugs and xenobiotics are known to induce changes in gene expression which are often more sensitive and characteristic than currently employed toxicological endpoints. We describe the use of quantitative real-time RT-PCR in the development of an in vitro -test to assess possible hazards of chemicals on endometrial functions essential for embryo implantation. Our work is part of the integrated project ReProTect (EU) developing new -in vitro_-tests which are required under the new European chemicals legislation (REACH) to reduce, refine or replace the use of laboratory animals. Within the ReProTect research area of “Implantation” we are exploring on the mRNA level predictive toxicological endpoints in human endometrial explants (e.g. leukaemia inhibitory factor, LIF; progesterone receptor; estrogen receptor α; calcitonin; cyclooxygenase-2; corticotrophin releasing hormone receptor 1; VEGF-receptor 2, KDR).

The goal of the human endometrial explants assay is to detect chemical effects on endometrial functions which are essential for embryo implantation. This test is a closer approach to in vivo -conditions than primary or permanent cell cultures. Endometrial tissues from the proliferative and secretory phase of the menstrual cycle are obtained by aspiration curettage from premenopausal women. The endometrial biopsies are chopped into pieces of 1-2 mm/side and cultured in sex steroid supplemented medium without phenol red in a humidified atmosphere at 37 °C in 5 % CO<sub>2 for 6-24 hrs. Test chemicals are administered during this incubation period and compared to negative controls with vehicle alone.

Facing the low tissue amounts of human endometrial explants which are available for each incubation (approximately 20 mg) quantitative real-time RT-PCR (LightCycler 480, Roche) is applied as the major analytical method. In order to identify predictive toxicological endpoints among a larger number of target genes assays from the highly versatile Universal Probe Library (UPL; Roche) are used. Evaluation is performed by calibrator-normalized relative quantification. A status report of our project will be presented. It includes calibrator standard curves for efficiency correction, selection of housekeeping genes and preliminary data of in vitro -testing with the antiprogestin reference compound RU 486.

This project is funded by the European Commission ( ReProTect , Project no.: LSHB-CT-2004-503257)


P 030

Borrelia burgdorferi sensu lato complex in Ixodes ricinus ticks in Slovenia and development of SYBR Green I melting curve analysis for separation between different borrelia genospecies.

Nataša Toplak1, Miha Kovač2, Minka Kovač1, Tjaša Cerar3 and Eva Ružić Sabljić3

1Omega d.o.o., Dolinškova 8, 1000 Ljubljana, 2Poljane Grammar School Gimnazija Poljane, Strossmayerjeva 1, 1000 Ljubljana and 3University of Ljubljana, Faculty of Medicine, Institute of Microbiology and Immunology, Zaloška 4, 1000 Ljubljana

Email: omega@omega.si

Worldwide, many infections caused by viruses, bacteria, or parasites are known to be tick-transmitted zoonoses. Tick-borne diseases are a major threat to mammals and humans during outdoor activities in spring and fall. One of the most important tick-borne diseases is Lyme borreliosis caused by spirochetes within the Borrelia burgdorferi sensu lato complex. The different species of this group are involved in clinical manifestat